Moreover, I have even more weaker peaks such as those exhibiting dynamics in solution and the carbon peaks are broad, and obviously I can pick up exactly 0 of them. This has never happened before and is extremely frustrating: it is there, clear as day, way above the noise, and i just can't pick it! I tried setting the "noise factor" to 0, setting the filter section to including "all" and excluding "none", and still cannot pick this peak out. Moreover, when i use manual peak select, i can't select it either. For example, in the 13C spectrum below, the carbonyl signal at 175 ppm is not picked up when i use automatic peak select. I have done this before for a paper, but it feels like MNova has gotten weird and frustrating and some signals are not reported. I am preparing some NMRs for reporting using MestReNova.
0 Comments
Leave a Reply. |
Details
AuthorWrite something about yourself. No need to be fancy, just an overview. ArchivesCategories |